Simultaneous mapping of EMCD signals and crystal orientations in a transmission electron microscope

نویسندگان

چکیده

Abstract When magnetic properties are analysed in a transmission electron microscope using the technique of circular dichroism (EMCD), one critical parameters is sample orientation. Since small orientation changes can have strong impact on measurement EMCD signal and such measurements need two separate conjugate EELS spectra, it experimentally non-trivial to measure as function Here, we developed methodology simultaneously map quantitative signals local crystal. We analyse, both by simulations, how measured evolve with change crystal tilt. Based this analysis, establish an accurate relationship between orientations signals. Our results demonstrate that variation tilt significantly alter strength signal. From optimisation orientation, obtain measurements.

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ژورنال

عنوان ژورنال: Scientific Reports

سال: 2021

ISSN: ['2045-2322']

DOI: https://doi.org/10.1038/s41598-021-81071-4